HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → Methylene-(2-methyl-2-thiophen-3-yl-propyl)-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | 2-Methyl-2-(thien-3-yl)propylamine | HCID 66722431 | — |
| Product | Methylene-(2-methyl-2-thiophen-3-yl-propyl)-amine | HCID 58117475 | — |
Reaction Steps
5.75 g (37.0 mmol) 2-methyl-2-thiophene-3-yl-propylamine and 3.61 mL (44.4 mmol) formaldehyde were stirred overnight at RT together with 2.0 g molecular sieve (4 Å powder). The reaction mixture was filtered and the filtrate was concentrated to dryness by rotary evaporation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08829006B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-51e055cce98b4aae868fcb60b4fa2906 |
| Source note | uspto-grants-2014_09 |