HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → Ethyl 2-(2-benzoyloxyethoxyimino)-4-chloro-3-oxobutyrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | 2-(2-Benzoyloxyethoxyimino)-3-oxobutyrate | HCID 86737192 | — |
| Product | Ethyl 2-(2-benzoyloxyethoxyimino)-4-chloro-3-oxobutyrate | HCID 53906646 | — |
Reaction Steps
A solution of 2-(2-benzoyloxyethoxyimino)-3-oxobutyrate (syn isomer, 28 g.), a sulfuryl chloride (13.5 g.) and acetic acid (30 ml.) was treated in a similar manner to that of Example A-(2) to give ethyl 2-(2-benzoyloxyethoxyimino)-4-chloro-3-oxobutyrate (syn isomer, 29 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04598147 |
| Source dataset | uspto-grants-1986_07 |
| ORD ID | ord-c34c0dfd72f443dbb411167f76aafaa3 |
| Source note | uspto-grants-1986_07 |