HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 58386742, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 5,6-Difluorooxindole | HCID 12585282 | — |
| Catalyst | Nickel | HCID 935 | — |
| Product | HCID 58386742 | HCID 58386742 | — |
Reaction Steps
1.5 g (9.0 mmol) 5,6-difluoro-1,3-dihydro-indol-2-one were stirred with 1.0 g Raney nickel in 50 mL methanol 3 h at 200° C. in an autoclave. The catalyst was filtered off and the filtrate was concentrated to dryness by rotary evaporation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08829006B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-6ca0e0dd9fcd45d8af65ab1cfe62807c |
| Source note | uspto-grants-2014_09 |