HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 12591561, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Hexadecyl-2.3-epoxypropylether | HCID 86740887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 12591561 | HCID 12591561 | — |
Reaction Steps
A cooled mixture of 15.5 g of methylamine, 50 cc. of tetrahydrofurane and 15 g of hexadecyl-2.3-epoxypropylether is heated to 60° C. for 2 hours in an autoclave, cooled and evaporated in a vacuo. The residue is purified by column chromatography (silicic acid gel//chloroform/methanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04599205 |
| Source dataset | uspto-grants-1986_07 |
| ORD ID | ord-b251f801dfc540c08ed8025e6bdc4c92 |
| Source note | uspto-grants-1986_07 |