反应详情

A cooled mixture of 15.5 g of methylamine, 50 cc. of tetrahydrofurane and 15 g of hexadecyl-2.3-epoxypropylether is heated to 60° C. for 2 hours in an autoclave, cooled and evaporated in a vacuo. The residue is purified by column chromatography (silicic acid gel//chloroform/methanol).

1. temperaturecooled
2. customevaporated in a vacuo
3. customThe residue is purified by column chromatography (silicic acid gel//chloroform/methanol)