Benzylamine → HCID 13386682, compound

HRID 745461Notes

Reaction equation

HRID 745461 reaction equation
[CH2:1]([NH2:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C([CH:25]1[O:49][CH:26]1[CH2:27][O:28][CH2:29][CH:30]1O[CH:31]1[CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44]CCC)CCCCCCCCCCCCCCC>O1CCCC1>[CH2:1]([NH:8][CH2:25][CH:26]([OH:49])[CH2:27][O:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH3:44])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 7504BenzylamineHCID 86740887HCID 86740887, compound

Product 1

HCID 13386682HCID 13386682, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

A mixture of 24.4 g of benzylamine, 100 cc. of tetrahydrofurane and 34 g of hexadecyl-2.3-epoxypropylether is refluxed for 8 hours and the solvent is evaporated in a vacuo. The residue is recrystallized from hexane.

Workup

  1. customthe solvent is evaporated in a vacuo
  2. customThe residue is recrystallized from hexane

Sources & evidence

ORD record
ord-f36aa69103cc4467b59b44ca2cd53308
Source dataset
uspto-grants-1986_07
Patent number
US04599205

Reaction notes

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