Hydrochloric Acid → HCID 13288294, compound

Participants

Reaction Steps

A solution of 66 mg of 1-(2-methylphenoxy)-3-[1,1,-dimethyl-2-(3-ethoxycarbonylhydrazino-6-pyridazinylamino)ethylamino]-2-propanol in 5 ml of 10% hydrochloric acid was refluxed for 5 hours. After the solvent was evaporated under reduced pressure, the residue was recrystallized from ethanol to give 31 mg of 1-(2-methylphenoxy)-3-[1,1-dimethyl-2-(3-hydrazino-6-pyridazinylamino)ethylamino]-2-propanol hydrochloride as colorless crystals.

Provenance & Evidence