Triphenylphosphine → HCID 23313744, Verbindung

Beteiligte Stoffe

Reaktionsschritte

Combine 15.0 g (0.086 mole) of 2-(4-chlorophenyl)ethyl chloride and 20.98 g (0.08 mole) of triphenylphosphine. Heat the mixture under a nitrogen atmosphere at 110°-120° C. for 3.5 days. Follow the progress of the reaction by thin layer chromatography on silica gel (hexanes). At the completion of the reaction triturate the resulting solid with 250 ml of anhydrous ether to afford the title compound.

Herkunft & Nachweise