HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Bromoethyl)-4-chlorobenzene → HCID 10754978, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Bromoethyl)-4-chlorobenzene | HCID 23029 | — |
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Product | HCID 10754978 | HCID 10754978 | — |
Reaction Steps
Combine 24.9 g (0.15 mole) of triethyl phosphite and 32.9 g of 2-(4-chlorophenyl)ethyl bromide. Heat the mixture at reflux under a nitrogen atmosphere for 5-6 hours. Distill the reaction mixture at reduced pressure (0.2 mm Hg) and collect the fraction distilling at 110°-148° C. to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04599344 |
| Source dataset | uspto-grants-1986_07 |
| ORD ID | ord-54f4ab5672da47789a3d5ce29e6c156d |
| Source note | uspto-grants-1986_07 |