反应详情

0.79 g (3.5 mmol) ethyl 2,3-dihydro-1H-indol-3-carboxylate were added batchwise at RT to 7.8 mL (7.8 mmol) of a 1 M lithium aluminium hydride solution (in THF) in 40 mL THF and refluxed for 1 h. Then the reaction mixture was combined with water while being cooled, the precipitate formed was filtered off and the filtrate was evaporated down.

1. temperaturerefluxed for 1 h
2. temperaturewhile being cooled
3. customthe precipitate formed
4. filtrationwas filtered off
5. customthe filtrate was evaporated down