HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bicarbonate → 2-(2-Aminoethoxyimino)-2-(2-formamidothiazol-4-yl)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | (2-Formamido-1,3-thiazol-4-yl)(oxo)acetic acid | HCID 13116693 | — |
| Reactant | 2-(O-aminooxy)ethylamine dihydrochloride | HCID 14362326 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-(2-Aminoethoxyimino)-2-(2-formamidothiazol-4-yl)acetic acid | HCID 54376671 | — |
Reaction Steps
To a solution of 2-(2-formamidothiazol-4-yl)glyoxylic acid (5.5 g.) in ethanol (100 ml. ) was added a solution of 2-(aminooxy)ethylamine.dihydrochloride (4.1 g.) in water (50 ml.). The resulting mixture was adjusted to pH 4 with an aqueous solution of sodium bicarbonate and stirred for 3 hours at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04599426 |
| Source dataset | uspto-grants-1986_07 |
| ORD ID | ord-9f3a6031062b4a48ada09d11faefac1b |
| Source note | uspto-grants-1986_07 |