HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → 2-Methyl-5-(pyrrolidinomethyl)thiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | 2-Methyl-5-(pyrrolidinocarbonyl)thiazole | HCID 23311723 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-Methyl-5-(pyrrolidinomethyl)thiazole | HCID 23506351 | — |
Reaction Steps
A solution of 2-methyl-5-(pyrrolidinocarbonyl)thiazole in dry ether was added dropwise to a suspension of lithium aluminium hydride and the mixture was stirred at room temperature to give the title compound as a colourless liquid, b.p. 61-62°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04600025 |
| Source dataset | uspto-grants-1986_07 |
| ORD ID | ord-9bada2e984af48fea3b3e4513a892e19 |
| Source note | uspto-grants-1986_07 |