HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23312160, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 53896129 | HCID 53896129 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23312160 | HCID 23312160 | 78.8% |
Reaction Steps
At room temperature and under normal pressure, 970 mg of 6-benzyloxycarbonyl-4-ethyl-β-carboline-3-carboxylic acid ethyl ester is hydrogenated for one hour in 50 ml of methanol with 3 ml of 1N hydrochloric acid and 1.50 g of 10% palladium/carbon. After the catalyst has been removed by filtration, the mixture is evaporated, thus obtaining 593 mg of 3-ethoxycarbonyl-4-ethyl-β-carboline-6-carboxylic acid as the hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04600715 |
| Source dataset | uspto-grants-1986_07 |
| ORD ID | ord-f9045f39492e478ca998565551e45680 |
| Source note | uspto-grants-1986_07 |