Hydrochloric Acid → HCID 23312314, compound
Reaction equation
[CH3:1][O:2][C:3]1[C:4]([O:18][CH3:19])=[CH:5][C:6]2[O:10][C:9]([CH:11]3[CH2:16][CH2:15][NH:14][CH2:13][CH2:12]3)=[CH:8][C:7]=2[CH:17]=1.Cl>>[CH3:1][O:2][C:3]1[C:4]([O:18][CH3:19])=[CH:5][C:6]2[O:10][C:9]([C:11]3[CH:12]=[CH:13][N:14]=[CH:15][CH:16]=3)=[CH:8][C:7]=2[CH:17]=1Participants
3
Procedure
Likewise analogously to Example 2, there is obtained, by hydrogenation of 12.5 g of 4-(5,6-dimethoxy-2-benzofuranyl)-pyridine, 4-(5,6-dimethoxy-2-benzofuranyl)-piperidine, M.P. 95-98, and its hydrochloride, M.P. 227°-229°.
Sources & evidence
- ORD record
- ord-bbc8111f65cd45bcb2de70e5f9d871a2
- Source dataset
- uspto-grants-1986_07
- Patent number
- US04600719
Reaction notes
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