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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 745859Generated: November 2, 2026

Sodium Carbonate → HCID 13375748, compound

https://huagongshe.com/reaction/745859

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium CarbonateHCID 10340—
ReactantHCID 13375747HCID 13375747—
SolventWaterHCID 962—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 13375748HCID 13375748—

Reaction Conditions

Temperature100 °C

Reaction Steps

6 g of 7-acetamido-4'-flavonecarboxylic acid methyl ester are dissolved in 600 cc of dioxane. 12 g of sodium carbonate, dissolved in 250 cc of water, are added and the mixture is heated at 100° C. with stirring until the reaction is complete, for about 8 hours. The reaction is checked by plate chromatography (benzene (90)-dioxane (25)-acetic acid (4) elution solvent).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04600788
Source datasetuspto-grants-1986_07
ORD IDord-5319e8221002439391d953dcfe835237
Source noteuspto-grants-1986_07