Sodium borohydride → HCID 23310928, compound

HRID 745893Notes

Reaction equation

HRID 745893 reaction equation
[BH4-].[Na+].[C:3]([CH:6]1[CH2:10][CH2:9][CH:8]([CH3:11])[C:7]1([CH3:14])[CH:12]=[O:13])([CH3:5])=[CH2:4]>C(O)(C)C>[C:3]([CH:6]1[CH2:10][CH2:9][CH:8]([CH3:11])[C:7]1([CH3:14])[CH2:12][OH:13])([CH3:5])=[CH2:4]

Participants

4

Reactant 2

HCID 4311764Sodium borohydrideHCID 233109291,2-Dimethyl-5-(prop-1-en-2-yl)cyclopentane-1-carbaldehyde

Product 1

HCID 23310928HCID 23310928, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

Into a 250 ml flask equipped with stirrer, thermometer reflux condensor, heating mantle and nitrogen blanket apparatus are placed 15 grams of sodium borohydride, 100 ml anhydrous isopropyl alcohol and 65 grams of 2-isopropenyl-1,5-dimethylcyclopentane carboxaldehyde having the structure: ##STR26## prepared according to U.S. Pat. No. 4,474,992 issued on Oct. 2, 1984.

Workup

  1. customInto a 250 ml flask equipped with stirrer
  2. temperaturethermometer reflux condensor, heating mantle and nitrogen blanket apparatus
  3. custom##STR26## prepared

Sources & evidence

ORD record
ord-bb0f43f23f4b4f94ab1524f8c3e67002
Source dataset
uspto-grants-1986_07
Patent number
US04601850

Reaction notes

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