Ethyl Acetate → HCID 70454371, compound

Participants

Reaction Steps

A solution of 31.2 g of N-[3-(2,4-dichlorophenyl)-2-methyl-2-prop-1-en-1-yl-propyl]-pyrrolidine and 27 g of crotyl bromide in 250 ml of ethyl acetate is refluxed for 5 hours. The mixture is then stirred for 15 hours at room temperature and the crystalline product which is obtained is filtered off, washed with ether and dried in vacuo. 15 g of the desired product is obtained; m.p.: 128° C.

Provenance & Evidence