HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Piperidone → 4-Oxo-N-propylpiperidine-1-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Piperidone | HCID 33721 | — |
| Reactant | Propyl isocyanate | HCID 61033 | — |
| Product | 4-Oxo-N-propylpiperidine-1-carboxamide | HCID 14571190 | — |
Reaction Steps
To piperid-4-one (11.8 g) was added n-propyl isocyanate in small portions at room temperature with stirring. After stirring 48 hr the solvent was removed in vacuo, and the residue was treated with diethyl ether, yielding (D.31) (19.1 g, 86%) as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04603138 |
| Source dataset | uspto-grants-1986_07 |
| ORD ID | ord-c1ed351b0df2415d906d4fc835725c64 |
| Source note | uspto-grants-1986_07 |