Hydrogen Peroxide → HCID 178488899, compound

HRID 746219Notes

Reaction equation

HRID 746219 reaction equation
Cl.Cl.[CH3:3][S:4][C:5]1[CH:6]=[C:7]([C:13]2[NH:14][C:15]3[CH:20]=[CH:19][N:18]=[CH:17][C:16]=3[N:21]=2)[CH:8]=[CH:9][C:10]=1[O:11][CH3:12].[OH:22]O>>[CH3:3][S:4]([C:5]1[CH:6]=[C:7]([C:13]2[NH:14][C:15]3[CH:20]=[CH:19][N:18]=[CH:17][C:16]=3[N:21]=2)[CH:8]=[CH:9][C:10]=1[O:11][CH3:12])=[O:22]

Participants

3

Reactant 2

HCID 784Hydrogen PeroxideHCID 178488898HCID 178488898, compound

Product 1

HCID 178488899HCID 178488899, compound

Procedure

The compound obtained in Example 34, was oxidised using hydrogen peroxide (2 eq) in a manner analogous to that described in Example 21. The title compound was obtained as a white solid, m.p. 227°-229° C.

Sources & evidence

ORD record
ord-f65a203dc5c84ead99b91a2bf8e597c4
Source dataset
uspto-grants-1986_07
Patent number
US04603139

Reaction notes

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