Dimethylamine → HCID 58591573, compound

Participants

Reaction Conditions

Reaction Steps

In a closed pressure vessel methanesulfonic acid 2-(6-methyl-benzo[b]thiophen-2-yl)-ethyl ester from the previous step was taken up in MeOH (30 mL) and a 40% solution of dimethylamine in MeOH (30 mL) was added. The mixture was stirred for 2 hours at 90° C., cooled down to room temperature and concentrated in vacuo to afford 3.55 g of dimethyl-[2-(6-methyl-benzo[b]thiophen-2-yl)-ethyl]-amine (97%).

Provenance & Evidence