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HRID746659

反应详情

EQUATION

反应方程式

HRID 746659 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)C(O)C(O)C(=O)O
HCID875

2,3-Dihydroxybutanedioic acid

C4H6O6

结构：Cc1ccc(O)c([C@H](CCN(C(C)C)C(C)C)c2ccccc2)c1
HCID443879

(R)-(+)-Tolterodine

C22H31NO

PRODUCTS

生成物

1
结构：Cc1ccc(O)c([C@H](CCN(C(C)C)C(C)C)c2ccccc2)c1.O=C(O)C(O)C(O)C(=O)O
HCID9847786

未命名化合物

收率 68.4%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

Tolterodine free base (5.0 gm) is dissolved in acetone (80 ml) and tartaric acid (3.0 gm) is added to the solution. Then the contents are stirred for 2 hours at 25° C. to 30° C. and filtered to give 5.0 gm of tolterodine tartrate form I.

WORKUP

后处理

  1. filtrationfiltered