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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 746788Generated: October 31, 2026

Hydrochloric Acid → HCID 69254967, compound

https://huagongshe.com/reaction/746788

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantSodium HydroxideHCID 14798—
ReactantHCID 58900184HCID 58900184—
SolventEthanolHCID 702—
ProductHCID 69254967HCID 69254967—

Reaction Steps

Add NaOH 2M (1 ml) to a suspension of 4′-[3-(propane-2-sulfonylamino)-thiophen-2-yl]-biphenyl-4-carboxylic acid ethyl ester (0.128 mmol) in ethanol (1 ml) and stir 24 h. Add 6N HCl until pH is approximately 1 and a white solid precipitates. Filter the solid to provide the title compound: MS (ES−): 400 (M−1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07393868B2
Source datasetuspto-grants-2008_07
ORD IDord-1f3b66bcfecb44029c68dce927aa8754
Source noteuspto-grants-2008_07