HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 69254967, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 58900184 | HCID 58900184 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69254967 | HCID 69254967 | — |
Reaction Steps
Add NaOH 2M (1 ml) to a suspension of 4′-[3-(propane-2-sulfonylamino)-thiophen-2-yl]-biphenyl-4-carboxylic acid ethyl ester (0.128 mmol) in ethanol (1 ml) and stir 24 h. Add 6N HCl until pH is approximately 1 and a white solid precipitates. Filter the solid to provide the title compound: MS (ES−): 400 (M−1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07393868B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-1f3b66bcfecb44029c68dce927aa8754 |
| Source note | uspto-grants-2008_07 |