Hydrochloric Acid → HCID 69205444, compound

Participants

Reaction Steps

1.59 g of compound (5), 10 ml of ethanol and 10 ml of 37% hydrochloric acid were mixed in a three-necked flask. The reaction medium was refluxed. The reaction was followed by TLC. When the starting product and the monoacetylated product disappeared, the mixture was allowed to return to ambient temperature. The precipitate was then filtered off, washed with water and then with diisopropyl ether, and dried under vacuum. 944 mg of a white powder (yield=73%) were obtained.

Provenance & Evidence