HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 69301372, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Reactant | HCID 22890902 | HCID 22890902 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 69301372 | HCID 69301372 | — |
Reaction Steps
A mixture of 4-fluoro-4′-hydroxy-1,1′-biphenyl-3-carbonitrile (0.50 g, 2.35×10−3 mol), 1-bromo-2-methoxyethane (0.33 g, 2.35×10−3 mol), potassium iodide (0.04 g, 2.35×10−4 mol) and potassium carbonate (1.30 g, 9.40×10−3 mol) in butanone (20 cm3) was reacted, worked up and purified as described for compound 3 in Example 2. Yield 0.26 g (40%), GC purity (100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07396487B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-f7cc0ad7a7bd4804bc118b652a6d4dec |
| Source note | uspto-grants-2008_07 |