Hydrochloric Acid → HCID 86611689, compound

Participants

Reaction Steps

tert-Butyl 4-(cyanamido(phenyl)methyl)piperazine-1-carboxylate (1.5 g) was dissolved in 16 ml of 2M HCl in dioxane. After four hours, the solution was diluted with dioxane (20 ml) and the solid, (phenyl(piperazin-1-yl)methylene)cyanamide hydrochloride (1 g), was collected via filtration. It was washed with ether before further use.

Provenance & Evidence