Phenyl Isothiocyanate → HCID 22350954, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of t-butyl 2-aminoethylcarbamate (1.76 ml) in ethanol (22 ml) was added dropwise phenyl isothiocyanate (1.5 g), and the mixture was heated at 75° C. for one hour. The reaction mixture was concentrated under reduced pressure and crystallized from n-hexane to give the title compound (3.25 g).

Provenance & Evidence