N,N-Dimethyl-1,3-propanediamine → HCID 22350930, compound

HRID 747534Notes

Reaction equation

HRID 747534 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[NH:7][C:8](=[S:12])SCC.[CH3:13][N:14]([CH3:19])[CH2:15][CH2:16][CH2:17][NH2:18]>C(O)C>[CH3:13][N:14]([CH3:19])[CH2:15][CH2:16][CH2:17][NH:18][C:8]([NH:7][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][N:1]=1)=[S:12]

Participants

4

Reactant 2

HCID 7993N,N-Dimethyl-1,3-propanediamineHCID 12214896Ethyl 2-Pyridyldithiocarbamate

Product 1

HCID 22350930HCID 22350930, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A mixture of ethyl 2-pyridyldithiocarbamate (600 mg), 3-(dimethylamino)propylamine (0.38 ml) and ethanol (6 ml) was heated with reflux under nitrogen atmosphere. One and half hour thereafter, the reaction mixture was concentrated under reduced pressure to give the title compound (786 mg) as crude oil.

Workup

  1. temperaturewas heated
  2. temperaturewith reflux under nitrogen atmosphere
  3. concentrationOne and half hour thereafter, the reaction mixture was concentrated under reduced pressure

Sources & evidence

ORD record
ord-c55300dbfc144f439c6f699b2f6b1245
Source dataset
uspto-grants-2008_07
Patent number
US07396842B2

Reaction notes

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