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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 747534Generated: October 30, 2026

N,N-Dimethyl-1,3-propanediamine → HCID 22350930, compound

https://huagongshe.com/reaction/747534

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN,N-Dimethyl-1,3-propanediamineHCID 7993—
ReactantEthyl 2-PyridyldithiocarbamateHCID 12214896—
SolventEthanolHCID 702—
ProductHCID 22350930HCID 22350930—

Reaction Steps

A mixture of ethyl 2-pyridyldithiocarbamate (600 mg), 3-(dimethylamino)propylamine (0.38 ml) and ethanol (6 ml) was heated with reflux under nitrogen atmosphere. One and half hour thereafter, the reaction mixture was concentrated under reduced pressure to give the title compound (786 mg) as crude oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07396842B2
Source datasetuspto-grants-2008_07
ORD IDord-c55300dbfc144f439c6f699b2f6b1245
Source noteuspto-grants-2008_07