HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 69315554, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 69311901 | HCID 69311901 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 69315554 | HCID 69315554 | — |
Reaction Steps
Morpholine (2.3 ml) was added to a solution of (3-chloromethyl-benzyl)-carbamic acid tert-butyl ester (Intermediate 5, 1.7 g) in THF (20 ml) and the mixture heated at reflux under nitrogen for 6 hours. Concentration of the reaction under vacuum gave N-tert-butyloxycarbonyl-3-(4-morpholinylmethyl)benzylamine (1.94 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07396843B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-e0cb96ba89454774b1096dedbc9747e1 |
| Source note | uspto-grants-2008_07 |