HRID747591

反应详情

EQUATION

反应方程式

HRID 747591 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To 5.3 g of (2-amino-5-chlorophenyl)(2-chlorophenyl)methanone dissolved in 50 ml of pyridine are added 5.29 g of 3,4-dimethoxybenzenesulfonyl chloride, and the mixture is left for 3 hours at room temperature. The reaction medium is concentrated, the residue is taken up in diisopropyl ether and the precipitate formed is filtered off to give, after drying, 5.2 g of the expected product.

WORKUP

后处理

  1. concentrationThe reaction medium is concentrated
  2. customthe precipitate formed
  3. filtrationis filtered off
  4. customto give
  5. customafter drying