HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12180674, compound → HCID 68567648, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12180674 | HCID 12180674 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68567648 | HCID 68567648 | 105.6% |
Reaction Steps
2.25 g of 1-methoxy-2-nitro-3-[(E)-2-phenylvinyl]benzene are added to 0.18 g of palladium-on-charcoal (10%) suspended in 90 ml of methanol, and placed under 4 bar of hydrogen. After 18 hours, the reaction medium is filtered through talc and the filtrate is concentrated to give 2.115 g of the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07396958B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-c85ba9d6cac945279cd0728e402c4a6a |
| Source note | uspto-grants-2008_07 |