Thionyl Chloride → 4-Phenylbenzoyl chloride

HRID 747701Notes

Reaction equation

HRID 747701 reaction equation
[C:1]1([C:7]2[CH:15]=[CH:14][C:10]([C:11](O)=[O:12])=[CH:9][CH:8]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.S(Cl)([Cl:18])=O>>[C:1]1([C:7]2[CH:15]=[CH:14][C:10]([C:11]([Cl:18])=[O:12])=[CH:9][CH:8]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 66724(1,1'-Biphenyl)-4-carboxylic acid

Product 1

HCID 841514-Phenylbenzoyl chloride

Procedure

10 ml of thionyl chloride as added to 1.05 g (5.3 mmol) of 4-phenylbenzoic acid, and they were heated under reflux for 3 hours. The solvent was evaporated to obtain the crude product.

Workup

  1. temperaturewere heated
  2. temperatureunder reflux for 3 hours
  3. customThe solvent was evaporated

Sources & evidence

ORD record
ord-877ec4f34c324bfeafbe6676597d361c
Source dataset
uspto-grants-2008_07
Patent number
US07396844B1

Reaction notes

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