HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Phenylbenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | (1,1'-Biphenyl)-4-carboxylic acid | HCID 66724 | — |
| Product | 4-Phenylbenzoyl chloride | HCID 84151 | — |
Reaction Steps
10 ml of thionyl chloride as added to 1.05 g (5.3 mmol) of 4-phenylbenzoic acid, and they were heated under reflux for 3 hours. The solvent was evaporated to obtain the crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07396844B1 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-877ec4f34c324bfeafbe6676597d361c |
| Source note | uspto-grants-2008_07 |