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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 747720Generated: October 29, 2026

Potassium Carbonate → HCID 54335254, compound

https://huagongshe.com/reaction/747720

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant3-CyanophenolHCID 13394—
ReactantHCID 54100368HCID 54100368—
SolventDimethylformamideHCID 6228—
ProductHCID 54335254HCID 54335254—

Reaction Steps

2.35 g (9.97 mmol) of t-butyl (1R)-2-chloro-1-(2-methylpropyl)ethylcarbamate was reacted with 2.42 g (20.3 mmol)) of 3-cyanophenol and 2.72 g (19.7 mmol) of potassium carbonate in dimethylformamide. After the treatment in an ordinary manner, the title compound was obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07396844B1
Source datasetuspto-grants-2008_07
ORD IDord-826b6dec0ba64686afc690c4b0e463b3
Source noteuspto-grants-2008_07