HRID747773

反应详情

EQUATION

反应方程式

HRID 747773 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

847 mg (2.43 mmol) of ethyl 4-(1-t-butoxycarbonyl-4-piperidyloxy)benzoate was dissolved in 50 ml of ethanol, and 5 ml of 1 N sodium hydroxide was added thereto, and they were stirred for 3 days. The reaction solution was concentrated and treated in an ordinary manner with ethyl acetate as the extractant to obtain the title compound.

WORKUP

后处理

  1. concentrationThe reaction solution was concentrated
  2. additiontreated in an ordinary manner with ethyl acetate as the extractant