HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroethylamine hydrochloride → 4-(N,N-Dimethylcarbamimidoyl)benzoic acid hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroethylamine hydrochloride | HCID 9793737 | — |
| Reactant | ethyl 4-(N,N-dimethylamidino)benzoate | HCID 22631319 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | 4-(N,N-Dimethylcarbamimidoyl)benzoic acid hydrochloride | HCID 53444509 | — |
Reaction Steps
Ethyl 4-(N,N-dimethylamidino)benzoate (compound of step 1 in Example 7) was heated under reflux in 6 N hydrochloric acid for 6 hours, and then the solvent was distilled off to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07396844B1 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-011748c33dcb4f3bb3746db45c807910 |
| Source note | uspto-grants-2008_07 |