huagongshe.com
HRID747786

反应详情

EQUATION

反应方程式

HRID 747786 的结构方程式

REACTANTS

反应物

2
结构：Cl.NCCCl
HCID9793737

2-Chloroethylamine hydrochloride

C2H7Cl2N

结构：CCOC(=O)c1ccc(C(=N)N(C)C)cc1
HCID22631319

Ethyl 4-[(dimethylamino)iminomethyl]benzoate

C12H16N2O2

PRODUCTS

生成物

1
结构：CN(C)C(=N)c1ccc(C(=O)O)cc1.Cl
HCID53444509

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cl
溶剂HCID313

Hydrochloric Acid

ClH

PROCEDURE

实验过程

Ethyl 4-(N,N-dimethylamidino)benzoate (compound of step 1 in Example 7) was heated under reflux in 6 N hydrochloric acid for 6 hours, and then the solvent was distilled off to obtain the title compound.

WORKUP

后处理

  1. distillationthe solvent was distilled off