Dimethylcarbamoyl Chloride → HCID 131726963, compound

Participants

Reaction Conditions

Reaction Steps

430 mg (1.58 mmol) of N-[2-(3-cyanophenoxy)ethyl]-piperidine-4-carboxyamide (JP2 19-1) was dissolved in 1.6 ml of dimethylformamide, and 0.3 ml (2.06 mmol) of triethylamine and 0.16 ml (1.74 mmol) of dimethyl carbamoyl chloride were added thereto at 0° C. and stirred at room temperature for 2 hours. It was treated in an ordinary manner with ethyl acetate as the extractant to obtain the title compound.

Provenance & Evidence