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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 747833Generated: October 30, 2026

Sulfuric Acid → HCID 21962143, compound

https://huagongshe.com/reaction/747833

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSulfuric AcidHCID 1118—
ReactantEthyl 3-(4-chlorophenyl)-3-oxopropanoateHCID 101336—
ReactantHCID 178485201HCID 178485201—
ProductHCID 21962143HCID 21962143—

Reaction Steps

The title compound was prepared from ethyl(4-chloro)benzoylacetate (5.0 g, 22 mmol) (obtained in preparation 2) and methylthiopseudourea.H2SO4 (3.31 g, 12 mmol) by following the procedure described in preparation 4, (0.573 g, 11.6%). MS m/z: 223 (M+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07399760B2
Source datasetuspto-grants-2008_07
ORD IDord-e1855d6e591343c1a674b647aeb18b96
Source noteuspto-grants-2008_07