HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → HCID 68594649, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | HCID 20552294 | HCID 20552294 | — |
| Product | HCID 68594649 | HCID 68594649 | 86% |
Reaction Steps
1-[1-(4-Methylbenzyl)-1H-1,2,4-triazol-5-yl]ethanol was synthesized in a manner similar to that of the procedure in Example 21B but using 1-(4-methylbenzyl)-1H-1,2,4-triazole and acetaldehyde as the starting materials. The product was isolated as a white solid in 86% yield. 1H NMR (400 MHz, DMSO-d6) δ 1.26 (d, 3H, J=6.9 Hz), 2.22 (s, 3H), 3.27 (s, 1H), 4.88-4.94 (m, 1H), 5.66 (d, 2H, J=5.91 Hz), 7.09 (s, 4H), 7.79 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07399778B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-207818bfa0ae4c9ea7c1e9e92e177053 |
| Source note | uspto-grants-2008_07 |