Potassium Carbonate → HCID 22939443, compound

HRID 748391Notes

Reaction equation

HRID 748391 reaction equation
C([O:4][CH2:5][CH2:6][CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[C:10]([C:14]#[N:15])[N:9]=1)(=O)C.C(=O)([O-])[O-].[K+].[K+]>CO>[OH:4][CH2:5][CH2:6][CH2:7][C:8]1[N:9]=[C:10]([C:14]#[N:15])[CH:11]=[CH:12][CH:13]=1

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 229393903-(6-Cyano-2-pyridyl)propyl acetate

Product 1

HCID 22939443HCID 22939443, compoundYield 92.3%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

3-(6-Cyano-2-pyridyl)propyl acetate (3.0 g, 14.7 mmol) was dissolved in methanol (15 ml), and potassium carbonate (0.08 g, 0.58 mmol) was added thereto. The reaction mixture was stirred at room temperature for 22 hrs and concentrated to give the titled compound (2.2 g, 92%).

Workup

  1. concentrationconcentrated

Sources & evidence

ORD record
ord-3ea673b917ad418ea742e738f8ee0f9e
Source dataset
uspto-grants-2008_07
Patent number
US07399759B2

Reaction notes

Loading…