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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 748443Generated: October 31, 2026

HCID 59750101, compound → HCID 59750357, compound

https://huagongshe.com/reaction/748443

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59750101HCID 59750101—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 59750357HCID 5975035782.2%

Reaction Conditions

Temperature0 °C

Reaction Steps

tert-Butyl [2-oxo-3-[2-(4-oxo-4H-1,3-benzothiazin-2-yl)-4-pyridyl]-1-imidazolidinyl]acetate (0.31 g, 0.70 mmol) was dissolved in trifluoroacetic acid (5 ml), and the mixture was stirred at 0° C. for 2 hrs. The solvent was evaporated and the residue was recrystallized from diethyl ether-methanol to give the titled compound (0.22 g, 81%) as white crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07399759B2
Source datasetuspto-grants-2008_07
ORD IDord-b5db8e7775c3420795c9d54e8798bd6b
Source noteuspto-grants-2008_07