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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 748474Generated: October 30, 2026

Trifluoroacetic acid → HCID 68458121, compound

https://huagongshe.com/reaction/748474

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 59750423HCID 59750423—
ProductHCID 68458121HCID 6845812185%

Reaction Steps

tert-Butyl 2-[2-(4-oxo-4H-1,3-benzothiazin-2-yl)-4-pyridyl]-1-pyrrolidinecarboxylate (0.35 g, 0.85 mmol) was dissolved in trifluoroacetic acid (5 ml), and the mixture was stirred at room temperature for 3 hrs. The solvent was evaporated, and the residue was recrystallized from diisopropyl ether-methanol to give the titled compound (0.31 g, 85%) as white crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07399759B2
Source datasetuspto-grants-2008_07
ORD IDord-1e0f688c337d480eae2733f4cd76ab1e
Source noteuspto-grants-2008_07