N,N-Dimethylethylenediamine → HCID 20117248, compound

HRID 748519Notes

Reaction equation

HRID 748519 reaction equation
[Cl:1][C:2]1[N:7]=[CH:6][C:5]([S:8](Cl)(=[O:10])=[O:9])=[CH:4][CH:3]=1.[CH3:12][N:13]([CH3:17])[CH2:14][CH2:15][NH2:16]>>[Cl:1][C:2]1[N:7]=[CH:6][C:5]([S:8]([NH:16][CH2:15][CH2:14][N:13]([CH3:17])[CH3:12])(=[O:10])=[O:9])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 66053N,N-DimethylethylenediamineHCID 27927922-Chloro-5-pyridinesulfonyl chloride

Product 1

HCID 20117248HCID 20117248, compoundYield 72%

Procedure

The title compound was prepared as described for Example 29 using 6-chloropyridine-3-sulfonylchloride and N,N-dimethylethane-1,2-diamine. Yield: 72%: MS (MS) m/z 264 (M++1).

Sources & evidence

ORD record
ord-3a0d9d3c76f94a218760c7936ef9b518
Source dataset
uspto-grants-2008_07
Patent number
US07399780B2

Reaction notes

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