HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bicarbonate Ion → 2,4-Dichloro-6-methoxy-3,5-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bicarbonate Ion | HCID 769 | — |
| Reactant | Cyanuric chloride | HCID 7954 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2,4-Dichloro-6-methoxy-3,5-triazine | HCID 19267 | — |
Reaction Steps
Cyanuric chloride was reacted with methanol in the presence of bicarbonate at 30° C. as described in the literature to give the product: mp 89-91° C. (lit mp 87-89° C., J. R. Dudley, et al, J. Amer. Chem. Soc., 1951, 73, 2986-2990), after recrystallization from heptane. 1H-NMR (CDCl3): δ4.12 (OCH3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07399841B1 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-5441bf5d396c40ae9ae40979705f8be2 |
| Source note | uspto-grants-2008_07 |