HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 87779354, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 22595510 | HCID 22595510 | — |
| Product | HCID 87779354 | HCID 87779354 | 92.2% |
Reaction Steps
To 1.0 g (4.1 mmol) of 2-(m-trifluoromethylbenzyl)butanoic acid was added 0.98 g (8.2 mol) of thionyl chloride, and the resulting mixture was refluxed for 3 hours. Thionyl chloride was removed by an evaporator to obtain 1.0 g of 2-(m-trifluoromethylbenzyl)butanoic acid chloride as a colorless liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07402548B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-07fe564620ef4023b369ae161162a2b2 |
| Source note | uspto-grants-2008_07 |