HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluorophenol → 2-Chloro-6-fluorophenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluorophenol | HCID 9707 | — |
| Reactant | Chlorine | HCID 24526 | — |
| Product | 2-Chloro-6-fluorophenol | HCID 2773710 | — |
Reaction Steps
4 g (56 mmol) of chlorine is introduced at this temperature. Then 60.5 g (540 mmol) of 2-fluorophenol are dropped in the solution over about 2 hours, while at the same rate 42 g (590 mmol) more chlorine is Introduced. After that 4 g more chlorine are introduced to complete the chlorination.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07402603B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-367a6d9629a04a91b3cfc3497a7bf7dc |
| Source note | uspto-grants-2008_07 |