HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 73877107, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 1-Propene, 1,3,3-trichloro- | HCID 117819 | — |
| Reactant | HCID 11286827 | HCID 11286827 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 73877107 | HCID 73877107 | 34.1% |
Reaction Steps
Using 0.37 g of (4-cyanobenzyl)malononitrile, 5 ml of N,N-dimethylformamide, 0.12 g of sodium hydride (60% in oil), and 0.25 g of 1,3,3-trichloropropene, and according to the process described in the Production Example 1, there was obtained 0.17 g of 2-(4-cyanobenzyl)-2-(3,3-dichloropropenyl)malononitrile (the present compound (56)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07402691B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-09504706476346d3a7a3bdbe91368c5c |
| Source note | uspto-grants-2008_07 |