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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 74963Generated: October 29, 2026

Lithium Hydroxide → HCID 67285599, compound

https://huagongshe.com/reaction/74963

Reaction equation

Participants

RoleNameHCIDCharge
ReactantLithium HydroxideHCID 3939—
ReactantMethanaminium, N-((dimethylamino)(3H-1,2,3-triazolo(4,5-b)pyridin-3-yloxy)methylene)-N-methyl-, hexafluorophosphate(1-) (1:1)HCID 9886157—
Reactant5-Chloro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-tosyl-1H-pyrrolo[2,3-b]pyridineHCID 57597747—
Reactant5-Chloro-3-(5-fluoro-4-methylsulfinyl-pyrimidin-2-yl)-1-(p-tolylsulfonyl)pyrrolo[2,3-b]pyridineHCID 67285321—
SolventPyridineHCID 1049—
SolventDimethylformamideHCID 6228—
SolventDichloromethaneHCID 6344—
ProductHCID 67285599HCID 67285599—

Reaction Steps

Amine, HATU, DMF; (b) BOC2O, NH4CO3H, pyridine, DMF; (c) i: Amine, HATU, DMF; then ii: 1N LiOH.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08829007B2
Source datasetuspto-grants-2014_09
ORD IDord-64c83f338c5745f887fbf6ee9e45da00
Source noteuspto-grants-2014_09