HuagongsheHuagongshe Chemistry Print Report · For research reference only
Beta-Nitrostyrene → HCID 59752542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Beta-Nitrostyrene | HCID 7626 | — |
| Reactant | 4-Methoxybenzylamine | HCID 75452 | — |
| Reactant | tert-Butyl 4-oxopiperidine-1-carboxylate | HCID 735900 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59752542 | HCID 59752542 | — |
Reaction Steps
The title compound (0.19 g) was prepared from 1.51 g of 4-oxo-piperidine-1-carboxylic acid tert-butyl ester, 1.0 mL of 4-methoxybenzylamine, and 1.13 g of (2-nitro-vinyl)-benzene, using EtOH as the solvent and omitting SiO2. MS (ESI): exact mass calculated for C21H22N2O, 318.17; found, m/z 319.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07402680B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-87ef6537d63c4eae8d2e09dfc3d60cd0 |
| Source note | uspto-grants-2008_07 |